{"id":25640,"date":"2016-09-14T06:03:01","date_gmt":"2016-09-14T13:03:01","guid":{"rendered":"https:\/\/hepatochem.com\/handle-hygroscopic-salts\/"},"modified":"2016-09-14T06:03:01","modified_gmt":"2016-09-14T13:03:01","slug":"handle-hygroscopic-salts","status":"publish","type":"post","link":"https:\/\/hepatochem.com\/euro\/handle-hygroscopic-salts\/","title":{"rendered":"How do you handle hygroscopic salts?"},"content":{"rendered":"<p><!DOCTYPE html PUBLIC \"-\/\/W3C\/\/DTD HTML 4.0 Transitional\/\/EN\" \"http:\/\/www.w3.org\/TR\/REC-html40\/loose.dtd\"><br \/>\n<html><body><\/p>\n<p>[et_pb_section fb_built=&#8221;1&#8243; admin_label=&#8221;section&#8221; _builder_version=&#8221;4.16&#8243; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_row admin_label=&#8221;row&#8221; _builder_version=&#8221;4.16&#8243; background_size=&#8221;initial&#8221; background_position=&#8221;top_left&#8221; background_repeat=&#8221;repeat&#8221; custom_margin=&#8221;-49px|auto||auto||&#8221; custom_padding=&#8221;0px|||0px||&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_column type=&#8221;4_4&#8243; _builder_version=&#8221;4.16&#8243; custom_padding=&#8221;|||&#8221; global_colors_info=&#8221;{}&#8221; custom_padding__hover=&#8221;|||&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_text admin_label=&#8221;Text&#8221; _builder_version=&#8221;4.18.0&#8243; background_size=&#8221;initial&#8221; background_position=&#8221;top_left&#8221; background_repeat=&#8221;repeat&#8221; hover_enabled=&#8221;0&#8243; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221; sticky_enabled=&#8221;0&#8243;]<\/p>\n<div align=\"justify\">Salts such as weak bases are omnipresent in organic chemistry. The conversion rate of a reaction can be greatly affected depending on the salt.While it is easy to weigh K<sub>2<\/sub>CO<sub>3<\/sub> or Na<sub>2<\/sub>CO<sub>3<\/sub>. Because salts like Cs<sub>2<\/sub>CO<sub>3<\/sub> or K<sub>3<\/sub>PO<sub>4<\/sub> are hydroscopic salts, they are more difficult to handle when the reaction conditions require anhydrous solution.<\/div>\n<div align=\"justify\"><\/div>\n<div align=\"justify\">\n<div align=\"center\"><b>No need for glove box<\/b><\/div>\n<div align=\"center\"><b><\/b><\/div>\n<div align=\"left\">When you want to test a hydroscopic salt you need to be able to weigh them in moisture free environment which requires the use of a isolation equipment such as a glove bag or a glove box. Because glove box is not common in organic synthesis laboratories; Therefore, chemists often pass on important salts such as potassium phosphate or cesium carbonate.<\/div>\n<div align=\"left\"><\/div>\n<div align=\"left\"><\/div>\n<div align=\"center\"><strong>Using pre-filled reaction vials<\/strong><\/div>\n<div align=\"center\"><\/div>\n<\/div>\n<div align=\"justify\">Pre-filled reaction vials allow to handle hydroscopic salts without the need for an isolation chamber. By simply injecting your reaction solution through the septum using a syringe you can try multiple salts and optimize your chemistry.<\/div>\n<div align=\"justify\"><\/div>\n<div align=\"justify\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-2603 size-medium\" title=\"hydroscopic salts\" src=\"https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-300x128.jpg\" alt=\"hydroscopic salts\" width=\"300\" height=\"128\" srcset=\"https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-300x128.jpg 300w, https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-600x256.jpg 600w, https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-768x328.jpg 768w, https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-1024x438.jpg 1024w, https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-scaled.jpg 1920w\" sizes=\"(max-width: 300px) 100vw, 300px\" \/><\/div>\n<div align=\"justify\"><\/div>\n<div align=\"justify\">We manufacture pre-filled incontrolledenvironmentand offerseveral vial formats that could fit any type of reaction setup. You can conveniently screen every relevant salts in one experiment.<\/div>\n<div>\n<div align=\"center\"><\/div>\n<div>\n<div align=\"center\"><strong>Reaction vials pre-filled with Cs<sub>2<\/sub>CO<sub>3<\/sub>, K<sub>2<\/sub>PO<sub>4<\/sub>, K<sub>2<\/sub>CO<sub>3<\/sub>, NaOAc, Na<sub>2<\/sub>CO<sub>3<\/sub>and NaHCO<sub>3<\/sub><\/strong><\/div>\n<\/div>\n<\/div>\n<ul>\n<li><strong>Reaction vials pre-filled with reagents and stir bar.<\/strong><\/li>\n<li><strong>Multiple format and vials available<\/strong><\/li>\n<li><strong>Microwave or conventional heating<\/strong><\/li>\n<li><strong>Pre-designed or custom arrays available<\/strong><\/li>\n<li><strong>Reagents are packaged under inert atmosphere<\/strong><\/li>\n<\/ul>\n<div><\/div>\n<div><\/div>\n<p><a href=\"\/evoluchem-screening-kits\/\" target=\"_blank\" rel=\"noopener noreferrer\" shape=\"rect\">Learn more about our kits<\/a><\/p>\n<p>[\/et_pb_text][\/et_pb_column][\/et_pb_row][\/et_pb_section]<\/body><\/html><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Salts such as weak bases are omnipresent in organic chemistry. The conversion rate of a reaction can be greatly affected depending on the salt.While it is easy to weigh K2CO3 or Na2CO3. Because salts like Cs2CO3 or K3PO4 are hydroscopic salts, they are more difficult to handle when the reaction conditions require anhydrous solution. No [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_et_pb_use_builder":"on","_et_pb_old_content":"<div align=\"justify\">Salts such as weak bases are omnipresent in organic chemistry. The conversion rate of a reaction can be greatly affected depending on the salt.\u00a0While it is easy to weigh K<sub>2<\/sub>CO<sub>3<\/sub> or Na<sub>2<\/sub>CO<sub>3<\/sub>, salts such as Cs<sub>2<\/sub>CO<sub>3<\/sub> or K<sub>3<\/sub>PO<sub>4<\/sub> are more difficult to handle when the reaction conditions require anhydrous solution.<\/div>\r\n<div align=\"justify\"><\/div>\r\n<div align=\"justify\">\r\n<div align=\"center\"><b>No need for glove box<\/b><\/div>\r\n<div align=\"center\"><b>\u00a0<\/b><\/div>\r\n<div align=\"left\">When you want to test a hydroscopic salt you need to be able to weigh them in moisture free environment which requires the use of a isolation equipment such as a glove bag or a glove box. Because glove box is not common in organic synthesis laboratories; Therefore, chemists often pass on important salts such as potassium phosphate or cesium carbonate.<\/div>\r\n<div align=\"left\"><\/div>\r\n<div align=\"left\"><\/div>\r\n<div align=\"center\"><strong>Using pre-filled reaction vials<\/strong><\/div>\r\n<div align=\"center\"><\/div>\r\n<\/div>\r\n<div align=\"justify\">Pre-filled reaction vials allow to handle hydroscopic salts without the need for an isolation chamber. By simply injecting your reaction solution through the septum using a syringe you can try multiple salts and optimize your chemistry.<\/div>\r\n<div align=\"justify\"><\/div>\r\n<div align=\"justify\"><img class=\"aligncenter size-medium wp-image-2603\" src=\"https:\/\/hepatochem.com\/wp-content\/uploads\/2016\/08\/IMAG0627-300x128.jpg\" alt=\"IMAG0627\" width=\"300\" height=\"128\" \/><\/div>\r\n<div align=\"justify\"><\/div>\r\n<div align=\"justify\">We manufacture pre-filled in\u00a0controlled\u00a0environment\u00a0and offer\u00a0several vial formats that could fit any type of reaction setup. You can conveniently screen every relevant salts in one experiment.<\/div>\r\n<div>\r\n<div align=\"center\"><\/div>\r\n<div>\r\n<div align=\"center\"><strong><a href=\"https:\/\/hepatochem.com\/chemistry-kits\/weak-base-kits\/\" target=\"_blank\" shape=\"rect\">Reaction vials pre-filled with Cs<sub>2<\/sub>CO<sub>3<\/sub>, K<sub>2<\/sub>PO<sub>4<\/sub>, K<sub>2<\/sub>CO<sub>3<\/sub>, NaOAc, Na<sub>2<\/sub>CO<sub>3<\/sub>\u00a0and NaHCO<sub>3<\/sub><\/a><\/strong><\/div>\r\n<\/div>\r\n<\/div>\r\n\u00a0\r\n<ul>\r\n \t<li><strong>Reaction vials pre-filled with reagents and stir bar.<\/strong><\/li>\r\n \t<li><strong>Multiple format and vials available<\/strong><\/li>\r\n \t<li><strong>Microwave or conventional heating<\/strong><\/li>\r\n \t<li><strong>Pre-designed or custom arrays available<\/strong><\/li>\r\n \t<li><strong>Reagents are packaged under inert atmosphere<\/strong><\/li>\r\n<\/ul>\r\n<div><\/div>\r\n<div><\/div>\r\n<a href=\"https:\/\/hepatochem.com\/chemistry-kits\/\" target=\"_blank\" shape=\"rect\">Learn more about our kits<\/a>\u00a0at\u00a0<a href=\"https:\/\/hepatochem.com\/chemistry-kits\/prefilled-reaction-vials\/\" target=\"_blank\" shape=\"rect\">https:\/\/hepatochem.com\/chemistry-kits\/prefilled-reaction-vials\/<\/a>","_et_gb_content_width":"","_jetpack_memberships_contains_paid_content":false,"footnotes":""},"categories":[680],"tags":[714,715,716],"class_list":["post-25640","post","type-post","status-publish","format-standard","hentry","category-featured-articles","tag-cesium","tag-hygroscopic","tag-salts"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v27.7 - https:\/\/yoast.com\/product\/yoast-seo-wordpress\/ -->\n<title>How do you handle hygroscopic salts?<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/hepatochem.com\/euro\/handle-hygroscopic-salts\/\" \/>\n<meta name=\"twitter:label1\" 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